Mohamed Jaffer, Sadiq MSamson, Nesaraj A.2023-09-132023-09-1320132170-161X2588-2082http://hdl.handle.net/123456789/15700Nickel oxide (NiO) nanoparticles were prepared by colloidal thermal assisted reflux condensation method using nickel acetate (precursor salt) and N, N - Dimethylformamide - DMF (solvent) with or without the addition of surfactants such as cetyl trimethyl ammonium bromide (CTAB), polyvinyl pyrrolidone (PVP), polyvinyl alcohol (PVA) and sodium monododecyl sulphate (SDS) respectively. Finally, the prepared samples products were calcined at different temperatures systematically such as at 200oC, 400oC, 600oC, 800oC for 2 hrs each to get the phase pure product. The calcined nanoparticles were characterized by X-Ray Diffraction (XRD), Energy Dispersive X-ray Analysis (EDAX), Fourier Transform Infrared (FTIR) Spectroscopy, Particle Size Analysis, Scanning Electron Microscopy (SEM), Diffuse Reflectance Spectroscopy (DRS) and Photo Luminescence (PL) Spectroscopy techniques. All the samples were crystallized in cubic structure. Effect of surfactants in the synthesis of nickel oxide (NiO) particles is discussed and reported.enThermal assisted reflux condensation methodNiO nanoparticlesEffect of surfactantsArticle